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where CR is the calculated concentration of the reference solution Some results are presented in Table 61 The apparent intrinsic solubilities Sapp , determined in this 0 way (eq 616) are listed in column 3, for the compounds used in one study All the Sapp values reported in Table 61 were determined in the presence of 05% v/v 0 DMSO, except for phenazopyridine, where 026% was used The results of a pH 4 95 solubility assay of chlorpromazine are shown in Fig 610 The horizontal line represents the upper limit of measurable solubility (eg, 125 mg/mL), which can be set by the instrument according to the requirements of the assay When the measured concentration reaches the line, the sample is completely dissolved, and solubility cannot be determined This is automatically determined by the instrument, based on the calculated value of R When measured points fall below the line, the concentration corresponds to the apparent solubility Sapp 6452 Cosolvent Method The sample plate is prepared as in the preceding method But before the spectra are taken, a volume Y of a water-miscible cosolvent is added to a volume Z of sample

In the example ow in Figure 551, the gsmSCF sends the ACR-GPRS result component and the following ACH-GPRS operation component in separate TC Continue messages The gsmSCF may, however, combine these two TCAP components in a single TC Continue message However, the ACR-GPRS Result component is governed by the operation timer associated with the ACR-GPRS operation, Tacrg (see 3GPP TS 29078 [106], section 8, for the operation timers) Before the gsmSCF can send the next ACH-GPRS operation, it may have to contact a charging database Hence, to prevent operation timer expiry in the gprsSSF, the gsmSCF may rst send TC Continue containing ACR-GPRS result, then contact the charging database and then send TC Continue containing the next ACH-GPRS If no new CAP ACH-GPRS arrives at the gprsSSF within a speci c time after the gprsSSF has sent ACR-GPRS, then the gprsSSF may close the CAMEL relationship This functionality may be compared with the Tccd timer in gsmSSF However, this functionality on the gprsSSF is optional, whereas the use of the Tccd timer in gsmSSF is mandatory This timer in gprsSSF should have a value that is longer than the TC guard timer 534 CAP v3 Operations for GPRS The present section provides an overview of the information ows used for GPRS control CAMEL phase 3 has dedicated sets of CAP v3 operations for the three main functionalities: call control, GPRS control and MO SMS control Table 521 lists the CAP v3 operations that are used for GPRS control For the contents of the individual operations, see 3GPP TS 23078 [83], sections 661 and 662 The ASN1 syntax of each operation and its argument is speci ed in 3GPP TS 29078 [106], section 5 The reader should further be aware that most parameters in the CAP operations for GPRS are syntactically marked optional The semantic rules of presence of each parameter in an operation are speci ed in the information ow descriptions in 3GPP TS 23078 [83] 535 On-line Charging for GPRS The on-line charging mechanism for GPRS uses mechanisms that are similar to the on-line charging mechanism that is used in call control A main parallel is the use of the CAP operations that are used for this purpose: Apply charging GPRS this operation is used by the gsmSCF to de ne a charging threshold in the gprsSSF Apply charging report GPRS this operation is used by the gprsSSF to report a charging event to the gsmSCF In principle, each charging threshold will lead to the subsequent reporting of a charging event, when that event occurs, unless the cancel GPRS operation is used to remove the charging thresholds from the gprsSSF.

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Massively parallel processors (MPP), which consist of processing nodes that don't share data (ie, shared-nothing) but compute by routing data between nodes Symmetric multiprocessing (SMP) machines, which consist of multiple processors that do share the same data Basically, any processor is free to use any data Clustered computing systems, which consist of multiple computers that typically don't share the same data but route it between computers over a network

Solubility ( g/mL)

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Figure 610 High-throughput solubility pH determination of chlorpromazine The horizontal line indicates the set upper limit of solubility, where the compound completely dissolves and solubility cannot be speci ed The points below the horizontal line are measured in the presence of precipitation and indicate solubility The solubility pH curve was collected in the presence of 05 vol% DMSO, and is affected by the cosolvent (see text) [Avdeef, A, Curr Topics Med Chem, 1, 277 351 (2001) Reproduced with permission from Bentham Science Publishers, Ltd]

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